23–26 Sept 2026
Metropol Lake Resort
Europe/Zurich timezone

Electrospun PLA/Tuff Composite Membranes: Fabrication, Structural Characterization, and Potential for Metal Adsorption

Not scheduled
15m
Metropol Lake Resort

Metropol Lake Resort

Naselba Dolno Konjsko bb, 6000 Ohrid, N. Macedonia
Oral presentation Polymers and polymer materials

Speaker

Aleksandra Ivanoska-Dacikj (Macedonian Academy of Sciences and Arts)

Description

Electrospinning enables the fabrication of micro- and nanofibrous materials with high surface area and porosity, making them attractive for water treatment and environmental remediation applications. In this study, electrospun polylactic acid (PLA) membranes containing 0, 2, 5, and 10 wt% natural opalized tuff were successfully fabricated and evaluated as eco-friendly adsorbents for heavy metals removal. The incorporation of tuff provided active mineral sites, while the PLA matrix ensured structural stability and biodegradability. Scanning electron microscopy (SEM) revealed a uniform fibrous morphology with well-developed porosity (Figure 1, left images). X-ray diffraction and Fourier-transform infrared spectroscopy confirmed the successful incorporation of tuff without altering the chemical structure of PLA. Energy Dispersive X-Ray (EDX) spectroscopy analysis demonstrated the effective adsorption of Ni2+ (Figure 1, right) and Pb2+ ions from aqueous solutions, indicating the important role of the silicate-rich mineral phase in the metal uptake.

Figure 1. SEM–EDX characterization of electrospun PLA-TUFF-0 and PLA-TUFF-10 membranes after 6 h exposure to Ni2+ solution.

The combination of a renewable polymer and a naturally occurring mineral filler resulted in porous composite membranes with promising adsorption performance.

Keywords: Electrospinning; Polylactic acid (PLA); Opalized tuff; Heavy metals adsorption, Biodegradable composites.

Author

Aleksandra Ivanoska-Dacikj (Macedonian Academy of Sciences and Arts)

Co-authors

Blažo Boev (Macedonian Academy of Sciences and Arts) Prof. Gligor Jovanovski (Macedonian Academy of Sciences and Arts) Prof. Gordana Bogoeva-Gaceva (Faculty of Technology and Metallurgy, Ss. Cyril and Methodius University in Skopje) Dr Maja Ristova Delipetrev (University “Goce Delchev” in Stip) Prof. Petre Makreski (Institute of Chemistry, Faculty of Natural Sciences and Mathematics, Ss. Cyril and Methodius University in Skopje)

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